Yes, we had an experiment of differential scanning calorimetry (DSC) to characterize the process, as shown in Figure 1. According to the result from DSC, there were an endothermic peak of phase transformation between the temperature range of 151~172 ℃, which are not exactly consistent with the results from in this paper. We think the difference in temperature is result from the different sample amount and heating rate. As with X-ray diffraction (XRD), the WAXS can be used to characterize the content of different phase in the phase transformation. So, we think the results in our paper is reasonable.
Materials and instruments, you need to specify the particle size of the initial CL-20 powders.